Ethane-1,2-diaminium 3,4,5,6-tetrabromo-2-(methoxycarbonyl)benzoate methanol solvate

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Ethane-1,2-diaminium 3,4,5,6-tetra­bromo-2-(methoxy­carbon­yl)benzoate methanol solvate

In the title compound, C(2)H(10)N(2) (2+)·2C(9)H(3)Br(4)O(4) (-)·CH(4)O, the N atoms of the ethane-1,2-diamine mol-ecule are protonated. The crystal structure is stabilized by N-H⋯O hydrogen bonds between the ethane-1,2-diaminium cations and 3,4,5,6-tetra-bromo-2-(methoxy-carbon-yl)bromo-benzoate anions, and by O-H⋯O and N-H⋯O hydrogen bonds between the methanol solvate and both the cation and ...

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The title compound, C(2)H(10)N(2) (2+)·2C(6)H(2)N(3)O(7) (-)·2H(2)O, crystallizes with a complete picrate anion and half an ethyl-enediammonium dication on a mirror plane, and two half-water mol-ecules (both on a mirror plane) in the asymmetric unit. The N atoms from separate half ethyl-enediammonium dications are in near proximity to a phenolate O atom and two o-NO(2) groups from the picrate a...

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[1,2-Bis(diphenyl­phosphino)ethane-κ2 P,P′](2-carboxyl­atothio­phenolato-κ2 O,S)nickel(II) methanol solvate

In the title complex, [Ni(C(7)H(4)O(2)S)(C(26)H(24)P(2))]·CH(3)OH, the nickel(II) centre adopts an approximately square-planar geometry, with the Ni atom coordinating to the S and O atoms of the bidentate thio-salicylate ligand and the two P atoms of the chelating Ph(2)PCH(2)CH(2)PPh(2) ligand. There is hydrogen bonding between the methanol solvent mol-ecule and the carbonyl O atom of the thio-...

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Ethane-1,2-diaminium 4,5-dichloro­phthalate

In the structure of the title compound, C(2)H(10)N(2) (2+)·C(8)H(2)Cl(2)O(4) (2-), the dications and dianions form hydrogen-bonded ribbon substructures which enclose conjoint cyclic R(2) (1)(7), R(1) (2)(7) and R(4) (2)(8) associations and extend down the c-axis direction. These ribbons inter-associate down b, giving a two-dimensional sheet structure. In the dianions, one of the carboxyl-ate gr...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2008

ISSN: 1600-5368

DOI: 10.1107/s1600536808038166